Great Britain were beaten 3-1 by Spain in their Davis Cup tie after Cameron Norrie lost in four sets to world number 21 Albert Ramos-Vinolas.

It was another superb effort from Norrie, ranked 114, but he finally lost 7-6 (7-4) 2-6 7-6 (7-4) 6-2 in three hours and 43 minutes in Marbella.

Kyle Edmund could have played in a deciding fifth rubber had Norrie won.

Britain now face a play-off in September which they need to win to stay in the World Group in 2019.

Norrie, 22, had come back from two sets down on Friday to defeat world number 23 Roberto Bautista Agut.

• Germany beat Australia in Davis Cup
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“I can’t speak highly enough of what Cam has done all weekend,” Great Britain captain Leon Smith said.

“People might have thought Friday was a one-off but he did it again against another high-quality player. He pushed him really close and I’m really proud of him.

“The only way is up for him.”

The first and third sets lasted 75 minutes and 76 minutes respectively with Norrie’s standard and energy levels finally dropping after he lost his second tie-break.

Ramos-Vinolas, who beat Liam Broady in the opening match of the tie on Friday, lost only two points on serve in the fourth set as he took Spain into April’s quarter-finals where they will face Germany.

Norrie impresses again but can’t keep the tie alive

While heavy favourites Spain ultimately prevailed, Norrie was the revelation of the weekend as he pushed two world-class clay-courters to the limit.

The Briton was quickly 4-0 down and faced two set points at 5-2 but somehow dragged himself to a tie-break in an incredible first set featuring eight breaks of serve.

A sensational pass from wide of the tramlines in the tie-break typified Norrie’s tenacity and inspiration but two errant forehands then cost him as Ramos-Vinolas closed out the first set.

The Briton would not go away though, holding from 0-30 down in his opening two service games of the second set, and winning five games in a row to level the match.

Norrie then fell 3-0 down in the third set but twice came back from a break down to force a second tie-break. Again, though, it was Ramos-Vinolas who took it with three Norrie errors in a row from 4-4 handing the Spaniard the set.

As well as Norrie played, he was never in front in the match and the effort of coming from behind finally told in the fourth set.

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German number one Alexander Zverev beat Nick Kyrgios in straight sets to give his country a 3-1 win over Australia in their Davis Cup World Group tie.

Zverev won 6-2 7-6 (7-3) 6-2 in Brisbane to put Germany into a quarter-final against Spain or Great Britain.

Kyrgios appeared troubled by an elbow problem and Zverev, the 20-year-old world number five, only faced two break points in the match.

“Hopefully this is just the beginning for us,” Zverev said.

“It’s awesome, it’s an amazing feeling and without my team-mates it wouldn’t have been possible.”

Kyrgios, 22, went into the match full of expectation after an impressive win over Jan-Lennard Struff in Friday’s opening singles.

His elbow problem became more noticeable as the game progressed, the Australian often shaking his right arm between points.

“It obviously affected me a lot,” Kyrgios said. “My serve is my biggest strength. I mean, I thought he played great today – but my serve was not really there and that affects the rest of my game.”

• GB’s Murray and Inglot beaten in doubles – report
• Live scores, schedule and results
• BBC coverage times

Zverev – who was pushed for almost four hours before seeing off 18-year-old Alex de Minaur in five sets on Friday – was rarely troubled.

Kyrgios lost two of his first four service games to surrender the opening set in just 23 minutes. He served better in the second set, firing down eight aces, but at 4-3 he had a medical timeout for treatment on his arm. The Australian continued to serve well and had two set points on Zverev’s serve at 6-5, but the German saved both then played a superb tiebreak to take a stranglehold on the match.

Defending champions France and fourth seeds Croatia lead 2-1 in their ties against the Netherlands and Canada respectively heading into Sunday.

Italy lead Japan and Belgium are 2-1 up against Hungary.

Germany took a 2-1 lead in their Davis Cup World Group tie against Australia after Tim Puetz and Jan-Lennard Struff won a tough five-set doubles rubber.

The duo beat John Peers and Matt Ebden 6-4 6-7 (1-7) 6-2 6-7 (4-7) 6-4 in three hours and 17 minutes in Brisbane.

German world number five Alexander Zverev will play Nick Kyrgios in the first singles rubber on Sunday.

Elsewhere, Ryan Harrison and Steve Johnson gave the United States an unassailable 3-0 lead in Serbia.

The Americans beat Nikola Milojevic and Miljan Zekic 6-7 (3-7) 6-2 7-5 6-4 in Nis to reach April’s quarter-finals, while Kazakhstan also secured their place in the last eight after their doubles victory over Switzerland in Astana.

Timur Khabibulin and Aleksandr Nedovyesov defeated Marc-Andrea Huesler and Luca Margaroli 6-4 6-4 3-6 6-7 (5-7) 6-3.

• GB’s Murray and Inglot beaten in doubles – report
• Live scores, schedule and results
• BBC coverage times

Defending champions France and fourth seeds Croatia both took 2-1 leads after victories in their respective doubles matches.

Pierre-Hugues Herbert joined up with Nicolas Mahut for France to beat Netherlands’ Robin Haase and Jean-Julien Rojer 7-6 (8-6) 6-3 6-7 (3-7) 7-6 (7-2) in Albertville.

Australian Open finalist Marin Cilic and Ivan Dodig came from two sets down to give hosts Croatia a 2-1 lead against Canada, defeating 45-year-old Daniel Nestor and Vasek Pospisil 2-6 3-6 6-4 7-5 6-2 in Osijek.

There was also a doubles win for Italy’s Simone Bolelli and Fabio Fognini, who beat beat Japan’s Ben McLachlan and Yasutaka Uchiyama in Morioka to go 2-1 up.

Hungary’s Marton Fucsovics and Attila Balazs held off a fightback from Belgium’s Joris de Loore and Ruben Bemelmans to win 6-3 6-4 6-7 (2-7) 4-6 7-5 in Liege and keep the tie alive with the hosts’ lead cut to 2-1.